INSTRUMENT CONTROL PARAMETERS: VOC_U --------------------------------------- D:\MassHunter\GCMS\1\methods\MSVOA_U.M Fri Aug 19 17:22:51 2022 Control Information ------- ----------- Sample Inlet : GC Injection Source : External Device Mass Spectrometer : Enabled No Sample Prep method has been assigned to this method. GC Oven Temperature Setpoint On (Initial) 45 °C Hold Time 4.07 min Post Run 70 °C Program #1 Rate 15 °C/min #1 Value 240 °C #1 Hold Time 0.6 min Equilibration Time 0.25 min Max Temperature 260 °C Maximum Temperature Override Enabled Slow Fan Disabled Cryo Off Front SS Inlet He Mode Split Heater On 220 °C Pressure On 14.909 psi Total Flow On 61.7 mL/min Septum Purge Flow On 5 mL/min Gas Saver On 15 After 1 min mL/min Split Ratio 80 :1 Split Flow 56 mL/min Thermal Aux 2 (MSD Transfer Line) Temperature Setpoint On (Initial) 250 °C Post Run 0 °C Column Column #1 Flow Setpoint Off (Initial) 0.7 mL/min Post Run 0.57353 mL/min Agilent 121-1324E DB-624 0 °C—280 °C (280 °C): 20 m x 180 μm x 1 μm Column lock Unlocked In Front SS Inlet He Out MSD (Initial) 45 °C Pressure 14.909 psi Flow 0.7 mL/min Average Velocity 37.252 cm/sec Holdup Time 0.89482 min Column Outlet Pressure 0 psi Signals Signal #1: Test Plot Description Test Plot Details Save Off Data Rate 50 Hz Dual Injection Assignment Front Sample Signal #2: Test Plot Description Test Plot Details Save Off Data Rate 50 Hz Dual Injection Assignment Back Sample Signal #3: Test Plot Description Test Plot Details Save Off Data Rate 50 Hz Dual Injection Assignment Back Sample Signal #4: Test Plot Description Test Plot Details Save Off Data Rate 50 Hz Dual Injection Assignment Back Sample MS Information -- ----------- General Information ------- ----------- Acquisition Mode : Scan Solvent Delay (minutes) : 1.25 Tune file : D:\MassHunter\GCMS\1\5977\061322LM.u EM Setting mode Gain : 1.500000 Normal or Fast Scanning : Normal Scanning Trace Ion Detection : On Run Time (if MS only) : 650 minutes [Scan Parameters] Start Time : 1.25 Low Mass : 35 High Mass : 300 Threshold : 100 A/D Samples: : 4 [MSZones] MS Source : 250 C maximum 250 C MS Quad : 170 C maximum 200 C Timed Events ----- ------ Number Events= 0 END OF MS ACQUISTION PARAMETERS TUNE PARAMETERS for SN: US1446L416 --------------------------------- Trace Ion Detection is ON. EMISSION : 34.593 ENERGY : 70.007 REPELLER : 33.305 IONFOCUS : 81.447 ENTRANCE_LE : 0.000 EMVOLTS : 1277.971 Actual EMV : 1503.9 GAIN FACTOR : 1.50 AMUGAIN : 1376.000 AMUOFFSET : 123.938 FILAMENT : 1.000 DCPOLARITY : 0.000 ENTLENSOFFS : 15.028 MASSGAIN : -518.000 MASSOFFSET : -36.000 END OF TUNE PARAMETERS ---------------------- END OF INSTRUMENT CONTROL PARAMETERS ------------------------------------