Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033303.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 09:37 Operator : UA\AJ Sample : PEM Misc : ALS Vial : 3 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 23 13:37:03 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 13:36:10 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.984 113.0E6 31427984 19.184 19.441 28) SA Decachlor... 8.101 9.007 154.1E6 31735261 19.800 20.573 Target Compounds 2) A alpha-BHC 3.838 4.363 82274509 20085399 8.919 9.274 3) MA gamma-BHC... 4.119 4.643 75203379 20055123 9.035 9.944 6) B beta-BHC 4.370 4.805 35758227 10016323 9.533 10.059 14) MA Endrin 5.919 6.659 400.0E6 73715950 49.892 48.938 17) MA 4,4'-DDT 6.285 7.082 818.5E6 145.4E6 112.532 112.041 20) A Methoxychlor 6.834 7.537 954.2E6 189.9E6 238.837 242.820 21) B Endrin ke... 7.057 7.666 4582461 751333 0.573m 0.498m --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.