Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033304.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 09:52 Operator : UA\AJ Sample : RESCHK Misc : ALS Vial : 4 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 23 13:37:16 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 13:36:10 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.984 118.0E6 32890242 20.034 20.346 28) SA Decachlor... 8.101 9.007 161.3E6 32774623 20.728 21.247 Target Compounds 9) A Endosulfan I 5.423 6.192 81756279 17721859 10.821 11.009 10) B gamma-Chl... 5.310 6.073 85397844 18041955 10.139m 10.244 12) B 4,4'-DDE 5.535 6.302 172.9E6 37259115 20.687m 20.760 13) MA Dieldrin 5.664 6.445 174.6E6 36202656 20.813 21.059 19) B Endosulfa... 6.572 7.207 151.4E6 29718404 20.837 20.852 20) A Methoxychlor 6.834 7.537 416.8E6 79652182 104.330 101.866 21) B Endrin ke... 7.058 7.670 170.4E6 27296560 21.304m 18.091 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.