Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033305.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  10:07
  Operator  : UA\AJ
  Sample    : PSTDICC100
  Misc      :  
  ALS Vial  : 5   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 23 11:30:48 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 11:29:59 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985   589.8E6  157.9E6   99.453    97.618  
28) SA  Decachlor...    8.102     9.009   726.3E6  140.8E6   92.777    91.672  

   Target Compounds
 2) A   alpha-BHC       3.839     4.364   961.1E6  224.4E6  101.223   101.734  
 3) MA  gamma-BHC...    4.120     4.645   869.4E6  205.6E6  100.908   100.797  
 4) MA  Heptachlor      4.408     5.159   887.3E6  191.4E6   98.978    98.470  
 5) MB  Aldrin          4.650     5.461   858.0E6  185.9E6  100.786    99.660  
 6) B   beta-BHC        4.371     4.806   375.4E6 95343238   99.455    96.045  
 7) B   delta-BHC       4.569     5.021   912.1E6  203.0E6  101.511   101.051  
 8) B   Heptachlo...    5.090     5.841   800.2E6  169.3E6   99.390   100.573  
 9) A   Endosulfan I    5.424     6.193   753.9E6  156.1E6   98.577    97.516  
10) B   gamma-Chl...    5.313     6.074   852.9E6  172.3E6   99.492    97.895  
11) B   alpha-Chl...    5.371     6.148   828.1E6  171.6E6   99.076    97.369  
12) B   4,4'-DDE        5.538     6.303   840.9E6  175.0E6   99.717    97.798  
13) MA  Dieldrin        5.665     6.447   857.5E6  170.2E6  100.112    98.777  
14) MA  Endrin          5.920     6.661   808.3E6  148.6E6   99.463    98.235  
15) B   Endosulfa...    6.193     6.863   757.8E6  144.0E6   98.607    96.352  
16) A   4,4'-DDD        6.050     6.783   697.4E6  132.7E6  100.600    98.323  
17) MA  4,4'-DDT        6.286     7.083   754.3E6  134.3E6  100.839   100.641  
18) B   Endrin al...    6.362     6.985   614.2E6  120.8E6   96.462    94.644  
19) B   Endosulfa...    6.572     7.208   704.9E6  135.7E6   97.190    95.735  
20) A   Methoxychlor    6.834     7.538   384.7E6 74342277   94.934    94.384  
21) B   Endrin ke...    7.060     7.671   789.5E6  147.0E6   96.670    96.233  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.