Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033306.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  10:22
  Operator  : UA\AJ
  Sample    : PSTDICC075
  Misc      :  
  ALS Vial  : 6   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 23 11:31:00 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 11:29:59 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985   442.9E6  119.0E6   74.679    73.538  
28) SA  Decachlor...    8.101     9.008   559.5E6  108.6E6   71.467    70.748  

   Target Compounds
 2) A   alpha-BHC       3.839     4.364   716.9E6  165.7E6   75.502    75.133  
 3) MA  gamma-BHC...    4.120     4.643   649.8E6  152.4E6   75.422    74.748  
 4) MA  Heptachlor      4.408     5.158   668.4E6  143.3E6   74.564    73.761  
 5) MB  Aldrin          4.650     5.460   640.2E6  138.0E6   75.208    74.021  
 6) B   beta-BHC        4.370     4.805   281.5E6 71976363   74.566    72.506  
 7) B   delta-BHC       4.569     5.020   679.5E6  150.9E6   75.622    75.140  
 8) B   Heptachlo...    5.090     5.840   601.2E6  126.2E6   74.682    74.969  
 9) A   Endosulfan I    5.423     6.193   569.2E6  117.3E6   74.418    73.271  
10) B   gamma-Chl...    5.312     6.073   641.3E6  129.2E6   74.815    73.382  
11) B   alpha-Chl...    5.371     6.147   622.9E6  129.0E6   74.521    73.170  
12) B   4,4'-DDE        5.537     6.302   631.2E6  131.4E6   74.848    73.449  
13) MA  Dieldrin        5.664     6.446   643.5E6  126.9E6   75.121    73.675  
14) MA  Endrin          5.919     6.660   608.1E6  111.2E6   74.829    73.499  
15) B   Endosulfa...    6.192     6.862   570.9E6  108.9E6   74.281    72.879  
16) A   4,4'-DDD        6.050     6.783   522.0E6 99288171   75.297    73.548  
17) MA  4,4'-DDT        6.286     7.082   563.1E6 99816123   75.270    74.788  
18) B   Endrin al...    6.361     6.984   471.0E6 92528329   73.967    72.522  
19) B   Endosulfa...    6.572     7.208   533.9E6  102.6E6   73.609    72.371  
20) A   Methoxychlor    6.834     7.537   294.3E6 56573133   72.634    71.825  
21) B   Endrin ke...    7.059     7.670   599.9E6  111.3E6   73.447    72.849  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.