Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033307.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  10:37
  Operator  : UA\AJ
  Sample    : PSTDICC050
  Misc      :  
  ALS Vial  : 7   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 23 11:30:20 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 11:29:59 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985   296.5E6 80899949   50.000    50.000  
28) SA  Decachlor...    8.101     9.008   391.4E6 76769517   50.000    50.000  

   Target Compounds
 2) A   alpha-BHC       3.839     4.364   474.8E6  110.3E6   50.000    50.000  
 3) MA  gamma-BHC...    4.119     4.644   430.8E6  102.0E6   50.000    50.000  
 4) MA  Heptachlor      4.407     5.158   448.2E6 97167731   50.000    50.000  
 5) MB  Aldrin          4.650     5.461   425.6E6 93244145   50.000    50.000  
 6) B   beta-BHC        4.370     4.805   188.7E6 49634423   50.000    50.000  
 7) B   delta-BHC       4.569     5.020   449.3E6  100.4E6   50.000    50.000  
 8) B   Heptachlo...    5.090     5.840   402.5E6 84157999   50.000    50.000  
 9) A   Endosulfan I    5.423     6.192   382.4E6 80039001   50.000    50.000  
10) B   gamma-Chl...    5.312     6.073   428.6E6 88005323   50.000    50.000  
11) B   alpha-Chl...    5.370     6.147   417.9E6 88121827   50.000    50.000  
12) B   4,4'-DDE        5.537     6.302   421.6E6 89481915   50.000    50.000  
13) MA  Dieldrin        5.664     6.446   428.3E6 86153171   50.000    50.000  
14) MA  Endrin          5.919     6.660   406.3E6 75635950   50.000    50.000  
15) B   Endosulfa...    6.192     6.862   384.3E6 74718365   50.000    50.000  
16) A   4,4'-DDD        6.050     6.783   346.6E6 67499136   50.000    50.000  
17) MA  4,4'-DDT        6.286     7.082   374.0E6 66732433   50.000    50.000  
18) B   Endrin al...    6.361     6.985   318.4E6 63792936   50.000    50.000  
19) B   Endosulfa...    6.572     7.208   362.6E6 70865300   50.000    50.000  
20) A   Methoxychlor    6.834     7.537   202.6E6 39382707   50.000    50.000  
21) B   Endrin ke...    7.059     7.670   408.4E6 76389011   50.000    50.000  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.