Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033308.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 10:52 Operator : UA\AJ Sample : PSTDICC025 Misc : ALS Vial : 8 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 23 11:31:12 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 11:29:59 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.984 146.1E6 40365863 24.640 24.948 28) SA Decachlor... 8.100 9.008 198.7E6 39580652 25.385 25.779 Target Compounds 2) A alpha-BHC 3.838 4.363 226.4E6 52490802 23.840 23.796 3) MA gamma-BHC... 4.119 4.643 205.3E6 49302135 23.824 24.174 4) MA Heptachlor 4.407 5.157 218.2E6 48046990 24.340 24.724 5) MB Aldrin 4.649 5.460 204.4E6 45731043 24.005 24.522 6) B beta-BHC 4.370 4.804 93291508 25062020 24.716 25.247 7) B delta-BHC 4.568 5.019 211.9E6 48461284 23.579 24.124 8) B Heptachlo... 5.090 5.839 200.5E6 41387539 24.911 24.589 9) A Endosulfan I 5.423 6.192 187.3E6 40064266 24.484 25.028 10) B gamma-Chl... 5.312 6.072 209.0E6 43834821 24.378 24.905 11) B alpha-Chl... 5.370 6.146 204.5E6 44125663 24.468 25.037 12) B 4,4'-DDE 5.536 6.301 205.6E6 44604692 24.385 24.924 13) MA Dieldrin 5.663 6.445 206.8E6 42497064 24.143 24.664 14) MA Endrin 5.920 6.659 197.2E6 37433305 24.267 24.746 15) B Endosulfa... 6.192 6.861 189.5E6 37374671 24.656 25.010 16) A 4,4'-DDD 6.049 6.782 166.3E6 33056608 23.992 24.487 17) MA 4,4'-DDT 6.286 7.082 177.9E6 32048377 23.784 24.013 18) B Endrin al... 6.361 6.984 158.2E6 32175264 24.850 25.219 19) B Endosulfa... 6.571 7.207 182.4E6 35809444 25.148 25.266 20) A Methoxychlor 6.833 7.537 101.2E6 19785872 24.969 25.120 21) B Endrin ke... 7.059 7.669 199.9E6 37871601 24.480 24.789 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.