Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033309.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 11:07 Operator : UA\AJ Sample : PSTDICC005 Misc : ALS Vial : 9 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 23 11:31:24 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 11:29:59 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.984 29402251 8421680 4.958 5.205 28) SA Decachlor... 8.100 9.008 42014504 8691841 5.367m 5.661 Target Compounds 2) A alpha-BHC 3.839 4.363 42009825 10350402 4.424 4.692 3) MA gamma-BHC... 4.119 4.643 37169697 9919854 4.314 4.864 4) MA Heptachlor 4.408 5.157 42086241 9974044 4.695 5.132 5) MB Aldrin 4.650 5.460 37997714 9424337 4.464 5.054 6) B beta-BHC 4.370 4.804 18713234 5351413 4.958 5.391 7) B delta-BHC 4.569 5.019 37644735 8623443 4.190 4.293 8) B Heptachlo... 5.090 5.839 39792270 7920222 4.943 4.706 9) A Endosulfan I 5.423 6.192 37551643 8602590 4.910 5.374 10) B gamma-Chl... 5.312 6.072 40512330 9235797 4.726 5.247 11) B alpha-Chl... 5.370 6.146 40978109 9505610 4.903 5.393 12) B 4,4'-DDE 5.537 6.301 41537610 9484515 4.926 5.300 13) MA Dieldrin 5.664 6.445 39727646 8890906 4.638 5.160 14) MA Endrin 5.920 6.659 39412256 7765041 4.850 5.133 15) B Endosulfa... 6.192 6.861 38759825 7976801 5.043 5.338 16) A 4,4'-DDD 6.050 6.781 32197720 6870738 4.645 5.090 17) MA 4,4'-DDT 6.286 7.081 33589544 5996967 4.490 4.493 18) B Endrin al... 6.362 6.983 33361081 6872206 5.239 5.386 19) B Endosulfa... 6.572 7.207 38100684 7759073 5.253 5.475 20) A Methoxychlor 6.834 7.535 20526436 4164081 5.065 5.287m 21) B Endrin ke... 7.059 7.669 39703732 7736559 4.861 5.064 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.