Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033310.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 11:22 Operator : UA\AJ Sample : PTOXICC1000 Misc : ALS Vial : 10 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 23 12:15:34 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\LTX022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 12:15:00 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticide 1 Signal #2 Phase: Rtx-CLPesticide 1 Signal #1 Info : 30M x 0.32mm x0.3 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.984 555.8E6 151.6E6 99.737 98.829 7) SA Decachlor... 8.101 9.008 691.2E6 137.1E6 97.321 93.970 Target Compounds 2) Toxaphene-1 5.627 6.350 42231875 8454662 1017.597 916.920 3) Toxaphene-2 6.469 7.038 128.7E6 14404846 1014.207 945.607 4) Toxaphene-3 6.820 7.117 105.9E6 39184971 980.939 950.146 5) Toxaphene-4 6.888 7.200 50155031 22269158 942.965 940.176 6) Toxaphene-5 6.950 7.605 145.6E6 18553670 1011.383 931.187 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.