Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033311.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 11:37 Operator : UA\AJ Sample : PTOXICC750 Misc : ALS Vial : 11 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 23 12:15:40 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\LTX022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 12:15:00 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticide 1 Signal #2 Phase: Rtx-CLPesticide 1 Signal #1 Info : 30M x 0.32mm x0.3 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.984 417.2E6 114.3E6 74.868 74.501 7) SA Decachlor... 8.101 9.007 523.4E6 105.5E6 73.687 72.320 Target Compounds 2) Toxaphene-1 5.628 6.350 31900096 6757551 768.648 732.866 3) Toxaphene-2 6.468 7.038 96361194 11025198 759.104 723.750 4) Toxaphene-3 6.820 7.116 77839887 29725338 720.970 720.771 5) Toxaphene-4 6.887 7.200 36287048 17243405 682.233 727.995 6) Toxaphene-5 6.950 7.604 115.3E6 14276098 800.949 716.500 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.