Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033312.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 11:52 Operator : UA\AJ Sample : PTOXICC500 Misc : ALS Vial : 12 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 23 12:15:13 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\LTX022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 12:15:00 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticide 1 Signal #2 Phase: Rtx-CLPesticide 1 Signal #1 Info : 30M x 0.32mm x0.3 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.985 278.6E6 76685831 50.000 50.000 7) SA Decachlor... 8.102 9.008 355.1E6 72949629 50.000 50.000 Target Compounds 2) Toxaphene-1 5.628 6.351 20750786 4610358 500.000 500.000 3) Toxaphene-2 6.468 7.039 63470382 7616721 500.000 500.000 4) Toxaphene-3 6.820 7.117 53982777 20620510 500.000 500.000 5) Toxaphene-4 6.888 7.200 26594335 11843079 500.000 500.000 6) Toxaphene-5 6.949 7.605 72001226 9962381 500.000 500.000 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.