Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033313.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 12:07 Operator : UA\AJ Sample : PTOXICC250 Misc : ALS Vial : 13 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 23 12:18:55 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\LTX022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 12:16:23 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticide 1 Signal #2 Phase: Rtx-CLPesticide 1 Signal #1 Info : 30M x 0.32mm x0.3 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.984 134.7E6 38188695 24.209 25.053 7) SA Decachlor... 8.102 9.007 178.9E6 37987699 25.564 26.898 Target Compounds 2) Toxaphene-1 5.628 6.350 10158584 2405804 241.360 270.462 3) Toxaphene-2 6.469 7.039 30529557 3811740 238.409 257.907 4) Toxaphene-3 6.820 7.117 25640744 10357123 242.153 258.799 5) Toxaphene-4 6.887 7.200 12349963 5731813 244.189m 249.403 6) Toxaphene-5 6.950 7.605 33654617 5242609 227.689 273.465 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.