Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033314.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 12:22 Operator : UA\AJ Sample : PCHLORICC1000 Misc : ALS Vial : 14 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 23 13:12:02 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 13:10:32 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.985 615.7E6 151.9E6 99.263 97.180 28) SA Decachlor... 8.102 9.009 686.8E6 138.0E6 94.737 93.902 Target Compounds 23) Chlordane-1 4.259 4.971 290.5E6 75557795 999.325 977.798 24) Chlordane-2 4.754 5.434 315.9E6 79565099 973.792 945.898 25) Chlordane-3 5.313 6.074 1038.0E6 263.0E6 1104.384 994.210 26) Chlordane-4 5.371 6.150 922.4E6 311.6E6 988.084 991.167 27) Chlordane-5 5.980 6.940 148.0E6 61082822 975.218 978.504 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.