Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033315.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 12:37 Operator : UA\AJ Sample : PCHLORICC750 Misc : ALS Vial : 15 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 23 13:12:11 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 13:10:32 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.985 454.0E6 113.8E6 73.197 72.778 28) SA Decachlor... 8.102 9.009 518.6E6 104.9E6 71.526 71.369 Target Compounds 23) Chlordane-1 4.259 4.971 212.7E6 55977314 731.902 724.406 24) Chlordane-2 4.755 5.434 235.5E6 60206226 725.895 715.753 25) Chlordane-3 5.314 6.074 766.3E6 194.1E6 815.327 733.580 26) Chlordane-4 5.371 6.150 682.1E6 229.7E6 730.733 730.481 27) Chlordane-5 5.979 6.941 114.7E6 45542158 756.208m 729.553 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.