Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033316.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 12:52 Operator : UA\AJ Sample : PCHLORICC500 Misc : ALS Vial : 16 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 23 13:10:57 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 13:10:27 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.985 310.1E6 78163434 50.000 50.000 28) SA Decachlor... 8.102 9.008 362.5E6 73485071 50.000 50.000 Target Compounds 23) Chlordane-1 4.259 4.971 145.3E6 38636697 500.000 500.000 24) Chlordane-2 4.754 5.434 162.2E6 42057979 500.000 500.000 25) Chlordane-3 5.311 6.074 468.9E6 132.3E6 498.898m 500.000 26) Chlordane-4 5.370 6.150 466.8E6 157.2E6 500.000 500.000 27) Chlordane-5 5.980 6.940 75867373 31212362 500.000 500.000 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.