Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033317.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 13:07 Operator : UA\AJ Sample : PCHLORICC250 Misc : ALS Vial : 17 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 23 13:27:03 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 13:13:39 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.985 148.1E6 38233194 24.137 24.938 28) SA Decachlor... 8.102 9.009 182.8E6 37716715 26.079 26.634 Target Compounds 23) Chlordane-1 4.259 4.971 69071896 18882471 239.603 249.035 24) Chlordane-2 4.755 5.433 79407051 21153014 249.601 260.125 25) Chlordane-3 5.312 6.073 265.2E6 63999223 265.247m 244.173 26) Chlordane-4 5.371 6.150 221.9E6 77112826 240.722 248.152 27) Chlordane-5 5.981 6.940 38673796 15199648 256.288 247.510 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.