Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033318.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 13:22 Operator : UA\AJ Sample : PCHLORICC050 Misc : ALS Vial : 18 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 23 13:33:49 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 13:28:48 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.401 3.984 29877973 8024699 4.911 5.237 28) SA Decachlor... 8.102 9.008 39406877 8184649 5.561 5.687 Target Compounds 23) Chlordane-1 4.259 4.969 13344865 3975386 46.778 52.481m 24) Chlordane-2 4.754 5.432 16580782 4263349 52.139 51.902m 25) Chlordane-3 5.313 6.073 46668146 13413814 45.975 51.477 26) Chlordane-4 5.370 6.149 42366382 16364528 46.391 52.759 27) Chlordane-5 5.980 6.938 8530290 3032597 56.176 49.506m --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.