Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033319.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 13:37 Operator : UA\AJ Sample : PSTDICV050 Misc : ALS Vial : 19 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 23 23:02:55 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 13:36:10 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.985 288.5E6 81020281 48.961 50.118 28) SA Decachlor... 8.102 9.009 382.0E6 77412196 49.095 50.184 Target Compounds 2) A alpha-BHC 3.840 4.364 460.1E6 110.9E6 49.876 51.214 3) MA gamma-BHC... 4.120 4.644 418.8E6 102.6E6 50.310 50.895 4) MA Heptachlor 4.408 5.158 436.1E6 97730719 49.671 50.455 5) MB Aldrin 4.651 5.461 416.5E6 94318712 50.295 50.829 6) B beta-BHC 4.371 4.805 183.6E6 49874543 48.945 50.089 7) B delta-BHC 4.570 5.019 436.5E6 103.9E6 50.557 53.452m 8) B Heptachlo... 5.091 5.840 382.3E6 83073358 47.735 50.056 9) A Endosulfan I 5.424 6.193 373.6E6 81027775 49.450 50.336 10) B gamma-Chl... 5.313 6.073 417.1E6 89141874 49.523 50.615 11) B alpha-Chl... 5.372 6.147 405.8E6 88767026 49.103 50.071 12) B 4,4'-DDE 5.538 6.302 410.9E6 90406227 49.167 50.374 13) MA Dieldrin 5.665 6.446 418.2E6 86853270 49.861 50.521 14) MA Endrin 5.920 6.660 397.5E6 76005653 49.582 50.458 15) B Endosulfa... 6.193 6.862 378.3E6 75727722 49.513 50.643 16) A 4,4'-DDD 6.051 6.783 335.5E6 68203119 49.403 50.916 17) MA 4,4'-DDT 6.288 7.083 366.3E6 68042743 50.369 52.421 18) B Endrin al... 6.363 6.985 312.8E6 65230727 49.190 51.133 19) B Endosulfa... 6.573 7.208 347.0E6 72128399 47.752 50.609 20) A Methoxychlor 6.835 7.538 200.2E6 39706933 50.121 50.781 21) B Endrin ke... 7.060 7.670 414.7E6 78164381 51.840 51.805 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.