Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033320.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 13:52 Operator : UA\AJ Sample : PTOXICV500 Misc : ALS Vial : 20 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 24 03:31:00 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\LTX022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 12:19:29 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : Rtx-CLPesticide 1 Signal #2 Phase: Rtx-CLPesticide 1 Signal #1 Info : 30M x 0.32mm x0.3 Signal #2 Info : 30M x 0.32mm x 0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.984 273.1E6 77319947 49.470 50.697 7) SA Decachlor... 8.102 9.009 359.1E6 74035591 51.031 51.446 Target Compounds 2) Toxaphene-1 5.627 6.351 21582784 4607908 517.259m 507.637 3) Toxaphene-2 6.469 7.039 62523842 7569511 493.982 508.144 4) Toxaphene-3 6.821 7.118 51058264 20094032 486.012 497.721 5) Toxaphene-4 6.889 7.201 23861215 11906079 474.552 518.367 6) Toxaphene-5 6.950 7.606 71359318 9137941 493.796 465.724 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.