Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033321.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 14:07 Operator : UA\AJ Sample : PCHLORICV500 Misc : ALS Vial : 21 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 23 23:03:15 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 13:36:10 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.985 297.8E6 76215259 50.545 47.146 28) SA Decachlor... 8.103 9.009 354.8E6 72480919 45.599 46.987 Target Compounds 23) Chlordane-1 4.259 4.971 139.9E6 37566403 496.877 491.057 24) Chlordane-2 4.755 5.434 157.2E6 41122435 490.111 496.846 25) Chlordane-3 5.313 6.074 503.6E6 128.4E6 504.223 489.874 26) Chlordane-4 5.371 6.150 445.6E6 153.4E6 495.087 489.134 27) Chlordane-5 5.981 6.940 72470430 30177552 465.748 493.612 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.