Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033323.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  14:37
  Operator  : UA\AJ
  Sample    : PEM
  Misc      :  
  ALS Vial  : 3   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 23 23:03:41 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985   109.9E6 31530179   18.658    19.504  
28) SA  Decachlor...    8.101     9.009   156.0E6 32836839   20.046    21.287  

   Target Compounds
 2) A   alpha-BHC       3.839     4.363  81044822 20201727    8.786     9.327  
 3) MA  gamma-BHC...    4.119     4.644  78407004 20224000    9.419    10.028  
 6) B   beta-BHC        4.371     4.805  36184273 10071031    9.646    10.114  
12) B   4,4'-DDE        5.535     6.299   1563991   119727    0.187m    0.067m#
14) MA  Endrin          5.920     6.661   386.5E6 74775786   48.210    49.642  
16) A   4,4'-DDD        6.053     6.783   1894677   497235    0.279m    0.371m#
17) MA  4,4'-DDT        6.286     7.083   798.4E6  148.3E6  109.773   114.273  
18) B   Endrin al...    6.360     6.983   1846521   348890    0.290m    0.273m 
20) A   Methoxychlor    6.834     7.538   952.8E6  193.6E6  238.486   247.598  
21) B   Endrin ke...    7.059     7.668   6007365  1630926    0.751     1.081m#
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.