Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033324.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  14:52
  Operator  : UA\AJ
  Sample    : PSTDCCC050
  Misc      :  
  ALS Vial  : 4   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 23 23:03:50 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985   294.5E6 82576189   49.977    51.081  
28) SA  Decachlor...    8.103     9.009   388.0E6 79094265   49.867    51.274  

   Target Compounds
 2) A   alpha-BHC       3.839     4.364   472.6E6  113.5E6   51.235    52.403  
 3) MA  gamma-BHC...    4.120     4.644   433.5E6  104.9E6   52.074    52.017  
 4) MA  Heptachlor      4.408     5.158   448.4E6 99230300   51.080    51.229  
 5) MB  Aldrin          4.650     5.461   429.4E6 96261301   51.859    51.876  
 6) B   beta-BHC        4.371     4.805   190.0E6 50957021   50.646    51.176  
 7) B   delta-BHC       4.569     5.019   450.6E6  104.7E6   52.195    53.909m 
 8) B   Heptachlo...    5.091     5.840   407.8E6 90605958   50.910    54.595  
 9) A   Endosulfan I    5.424     6.193   385.0E6 82844021   50.964    51.464  
10) B   gamma-Chl...    5.313     6.073   430.8E6 91518711   51.147    51.965  
11) B   alpha-Chl...    5.371     6.147   418.4E6 90813799   50.623    51.226  
12) B   4,4'-DDE        5.538     6.303   426.9E6 92260418   51.077    51.407  
13) MA  Dieldrin        5.665     6.446   432.4E6 88961400   51.557    51.747  
14) MA  Endrin          5.921     6.661   406.1E6 77280062   50.650    51.304  
15) B   Endosulfa...    6.193     6.863   387.4E6 77900809   50.701    52.096  
16) A   4,4'-DDD        6.051     6.783   347.9E6 69847553   51.224    52.144  
17) MA  4,4'-DDT        6.287     7.083   374.8E6 69104310   51.537    53.239  
18) B   Endrin al...    6.363     6.984   321.6E6 66186529   50.578    51.882  
19) B   Endosulfa...    6.573     7.208   367.5E6 73765322   50.569    51.758  
20) A   Methoxychlor    6.835     7.538   204.9E6 40316021   51.293    51.560  
21) B   Endrin ke...    7.061     7.671   426.2E6 79785588   53.270    52.879  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.