Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033325.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  15:07
  Operator  : UA\AJ
  Sample    : PB106716BS
  Misc      :  
  ALS Vial  : 5   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 23 23:04:03 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985  96993877 28515453   16.462    17.639  
28) SA  Decachlor...    8.102     9.009   141.2E6 29869894   18.154    19.364  

   Target Compounds
 2) A   alpha-BHC       3.839     4.364   524.0E6  126.0E6   56.810    58.192  
 3) MA  gamma-BHC...    4.120     4.644   478.8E6  116.1E6   57.519    57.565  
 4) MA  Heptachlor      4.408     5.159   497.1E6  109.9E6   56.629    56.746  
 5) MB  Aldrin          4.650     5.461   473.8E6  106.4E6   57.215    57.327  
 6) B   beta-BHC        4.371     4.805   211.0E6 56218199   56.254    56.460  
 7) B   delta-BHC       4.569     5.019   504.0E6  118.7E6   58.379    61.118m 
 8) B   Heptachlo...    5.090     5.841   457.3E6 98197971   57.090    59.170  
 9) A   Endosulfan I    5.424     6.194   426.2E6 91631140   56.409    56.923  
10) B   gamma-Chl...    5.313     6.074   477.5E6  100.3E6   56.688    56.956  
11) B   alpha-Chl...    5.371     6.148   463.0E6  100.2E6   56.020    56.527  
12) B   4,4'-DDE        5.537     6.303   466.2E6  101.9E6   55.779    56.775  
13) MA  Dieldrin        5.664     6.447   479.8E6 98260270   57.206    57.156  
14) MA  Endrin          5.920     6.661   451.3E6 85915743   56.283    57.037  
15) B   Endosulfa...    6.193     6.863   432.4E6 85807240   56.584    57.383  
16) A   4,4'-DDD        6.050     6.784   387.0E6 77556264   56.982    57.899  
17) MA  4,4'-DDT        6.287     7.083   416.2E6 76453335   57.228    58.900  
18) B   Endrin al...    6.362     6.986   360.7E6 73915952   56.733    57.941  
19) B   Endosulfa...    6.573     7.208   411.1E6 81686947   56.564    57.316  
20) A   Methoxychlor    6.835     7.538   226.7E6 44602690   56.745    57.042  
21) B   Endrin ke...    7.060     7.671   474.6E6 88665468   59.330    58.764  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.