Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033329.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  16:08
  Operator  : UA\AJ
  Sample    : J1619-01MS
  Misc      :  
  ALS Vial  : 9   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 23 23:04:36 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985  96393599 29183682   16.360    18.053  
28) SA  Decachlor...    8.102     9.009   148.4E6 32014436   19.072    20.754  

   Target Compounds
 2) A   alpha-BHC       3.839     4.363   539.7E6  141.8E6   58.511    65.462  
 3) MA  gamma-BHC...    4.120     4.644   492.3E6  126.2E6   59.147    62.553  
 4) MA  Heptachlor      4.408     5.158   499.2E6  114.5E6   56.859    59.132  
 5) MB  Aldrin          4.650     5.460   402.6E6  110.6E6   48.624    59.587  
 6) B   beta-BHC        4.373     4.805   302.1E6 58529207   80.526    58.781 #
 7) B   delta-BHC       4.569     5.018   499.4E6  152.8E6   57.844    78.671m#
 8) B   Heptachlo...    5.090     5.840   459.0E6  103.1E6   57.307    62.103  
 9) A   Endosulfan I    5.424     6.193   435.0E6 96375831   57.576    59.870  
10) B   gamma-Chl...    5.313     6.073   491.7E6  106.0E6   58.383    60.203  
11) B   alpha-Chl...    5.371     6.147   481.3E6  104.6E6   58.244    58.978  
12) B   4,4'-DDE        5.537     6.303   456.4E6  103.9E6   54.608    57.867  
13) MA  Dieldrin        5.665     6.446   477.2E6  100.7E6   56.891    58.574  
14) MA  Endrin          5.920     6.660   462.5E6 87114450   57.691    57.833  
15) B   Endosulfa...    6.193     6.861   388.3E6 93172042   50.819    62.308m 
16) A   4,4'-DDD        6.051     6.783   355.1E6 79860603   52.288    59.619  
17) MA  4,4'-DDT        6.287     7.081   405.0E6 82724927   55.685    63.732m 
18) B   Endrin al...    6.363     6.983   346.9E6 74338296   54.558    58.272m 
19) B   Endosulfa...    6.573     7.208   408.1E6 85063903   56.160    59.686  
20) A   Methoxychlor    6.835     7.537   219.5E6 46170913   54.936    59.048  
21) B   Endrin ke...    7.060     7.670   477.0E6 92079405   59.629    61.027  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.