Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033330.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  16:23
  Operator  : UA\AJ
  Sample    : J1619-01MSD
  Misc      :  
  ALS Vial  : 10   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 23 23:04:49 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985  99159447 28621904   16.830    17.705  
28) SA  Decachlor...    8.103     9.009   148.1E6 31858516   19.038    20.653  

   Target Compounds
 2) A   alpha-BHC       3.839     4.364   534.5E6  141.3E6   57.946    65.261  
 3) MA  gamma-BHC...    4.120     4.644   488.7E6  126.5E6   58.712    62.742  
 4) MA  Heptachlor      4.408     5.158   493.7E6  114.4E6   56.240    59.040  
 5) MB  Aldrin          4.651     5.461   400.2E6  110.0E6   48.331    59.255  
 6) B   beta-BHC        4.373     4.805   302.0E6 58581866   80.522    58.834 #
 7) B   delta-BHC       4.569     5.018   492.1E6  154.7E6   57.002    79.620m#
 8) B   Heptachlo...    5.091     5.840   454.8E6  102.8E6   56.783    61.950  
 9) A   Endosulfan I    5.424     6.193   433.0E6 96229416   57.312    59.779  
10) B   gamma-Chl...    5.313     6.074   482.1E6  104.5E6   57.241    59.341  
11) B   alpha-Chl...    5.371     6.147   475.8E6  104.3E6   57.576    58.848  
12) B   4,4'-DDE        5.537     6.303   451.5E6  103.4E6   54.016    57.605  
13) MA  Dieldrin        5.665     6.447   472.7E6  100.3E6   56.363    58.356  
14) MA  Endrin          5.921     6.660   458.6E6 87671333   57.193    58.203  
15) B   Endosulfa...    6.193     6.862   385.0E6 92684212   50.378    61.982m 
16) A   4,4'-DDD        6.051     6.783   350.5E6 79557912   51.607    59.393  
17) MA  4,4'-DDT        6.287     7.082   402.4E6 83743810   55.322    64.517m 
18) B   Endrin al...    6.363     6.984   342.9E6 74014538   53.936    58.018m 
19) B   Endosulfa...    6.574     7.208   402.0E6 84704093   55.321    59.433  
20) A   Methoxychlor    6.835     7.538   215.7E6 46001380   54.000    58.831  
21) B   Endrin ke...    7.061     7.671   452.5E6 91998127   56.559    60.973  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.