Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033333.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  17:08
  Operator  : UA\AJ
  Sample    : PB106757BS
  Misc      :  
  ALS Vial  : 13   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 23 23:09:34 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985  91770777 26913849   15.576    16.649  
28) SA  Decachlor...    8.102     9.010   131.8E6 28070261   16.938    18.197  

   Target Compounds
 2) A   alpha-BHC       3.839     4.364   491.9E6  119.8E6   53.330    55.334  
 3) MA  gamma-BHC...    4.119     4.644   448.8E6  110.7E6   53.912    54.904  
 4) MA  Heptachlor      4.408     5.158   466.7E6  105.2E6   53.165    54.311  
 5) MB  Aldrin          4.650     5.461   443.2E6  101.3E6   53.524    54.577  
 6) B   beta-BHC        4.371     4.805   198.3E6 53623384   52.857    53.854  
 7) B   delta-BHC       4.569     5.019   473.4E6  113.1E6   54.829    58.226m 
 8) B   Heptachlo...    5.090     5.839   426.8E6 97296193   53.280    58.627m 
 9) A   Endosulfan I    5.424     6.193   396.1E6 86809759   52.432    53.927  
10) B   gamma-Chl...    5.313     6.074   440.6E6 94939695   52.306    53.907  
11) B   alpha-Chl...    5.371     6.148   428.5E6 94947889   51.845    53.558  
12) B   4,4'-DDE        5.538     6.303   431.8E6 96412193   51.664    53.720  
13) MA  Dieldrin        5.664     6.447   441.9E6 93041477   52.686    54.121  
14) MA  Endrin          5.921     6.661   420.4E6 80936925   52.430    53.732  
15) B   Endosulfa...    6.193     6.863   395.4E6 81727331   51.750    54.655  
16) A   4,4'-DDD        6.050     6.784   354.8E6 73553002   52.246    54.910  
17) MA  4,4'-DDT        6.287     7.084   374.5E6 71872072   51.495    55.371  
18) B   Endrin al...    6.362     6.986   328.9E6 69870653   51.731    54.770  
19) B   Endosulfa...    6.573     7.209   371.9E6 77206846   51.175    54.173  
20) A   Methoxychlor    6.835     7.539   205.1E6 42004824   51.325    53.720  
21) B   Endrin ke...    7.061     7.671   430.3E6 83639959   53.784    55.434  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.