Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033336.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  17:53
  Operator  : UA\AJ
  Sample    : J1396-02MS
  Misc      :  
  ALS Vial  : 16   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 23 23:10:15 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985   112.1E6 32510641   19.028    20.111  
28) SA  Decachlor...    8.102     9.010   154.0E6 32328196   19.789    20.957  

   Target Compounds
 2) A   alpha-BHC       3.839     4.364   565.4E6  137.4E6   61.290    63.455  
 3) MA  gamma-BHC...    4.120     4.644   511.4E6  127.3E6   61.440    63.139  
 4) MA  Heptachlor      4.409     5.158   523.3E6  118.0E6   59.613    60.904  
 5) MB  Aldrin          4.650     5.460   501.4E6  114.3E6   60.550    61.593  
 6) B   beta-BHC        4.371     4.805   225.1E6 60209847   60.009    60.469  
 7) B   delta-BHC       4.569     5.018   543.5E6  132.7E6   62.953    68.326m 
 8) B   Heptachlo...    5.091     5.839   477.3E6  109.3E6   59.587    65.840m 
 9) A   Endosulfan I    5.424     6.193   449.3E6 98491337   59.468    61.184  
10) B   gamma-Chl...    5.313     6.074   503.4E6  107.8E6   59.767    61.214  
11) B   alpha-Chl...    5.371     6.147   486.8E6  107.3E6   58.906    60.518  
12) B   4,4'-DDE        5.537     6.303   490.4E6  109.1E6   58.679    60.808  
13) MA  Dieldrin        5.665     6.447   508.9E6  106.1E6   60.673    61.722  
14) MA  Endrin          5.921     6.661   482.7E6 92600060   60.203    61.475  
15) B   Endosulfa...    6.193     6.863   453.8E6 92533158   59.394    61.881  
16) A   4,4'-DDD        6.051     6.784   405.3E6 83015765   59.679    61.974  
17) MA  4,4'-DDT        6.287     7.083   431.4E6 82122197   59.309    63.268  
18) B   Endrin al...    6.363     6.986   371.6E6 78783109   58.442    61.756  
19) B   Endosulfa...    6.573     7.209   428.6E6 88336755   58.980    61.982  
20) A   Methoxychlor    6.835     7.539   232.8E6 46958048   58.271    60.054  
21) B   Endrin ke...    7.061     7.671   490.7E6 95440639   61.336    63.255  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.