Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033337.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  18:08
  Operator  : UA\AJ
  Sample    : J1396-02MSD
  Misc      :  
  ALS Vial  : 17   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 23 23:10:32 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985   115.6E6 33186500   19.628    20.529  
28) SA  Decachlor...    8.103     9.010   152.2E6 32868977   19.557    21.308  

   Target Compounds
 2) A   alpha-BHC       3.839     4.364   578.6E6  139.8E6   62.724    64.551  
 3) MA  gamma-BHC...    4.119     4.644   524.9E6  129.3E6   63.057    64.099  
 4) MA  Heptachlor      4.408     5.158   535.3E6  119.3E6   60.979    61.580  
 5) MB  Aldrin          4.650     5.461   509.9E6  116.0E6   61.578    62.490  
 6) B   beta-BHC        4.371     4.806   232.3E6 61197436   61.941    61.461  
 7) B   delta-BHC       4.569     5.019   553.0E6  135.3E6   64.048    69.632m 
 8) B   Heptachlo...    5.091     5.839   493.1E6  113.0E6   61.557    68.100m 
 9) A   Endosulfan I    5.424     6.193   453.0E6  100.1E6   59.962    62.185  
10) B   gamma-Chl...    5.313     6.074   515.3E6  109.3E6   61.179    62.081  
11) B   alpha-Chl...    5.371     6.148   495.1E6  108.5E6   59.911    61.218  
12) B   4,4'-DDE        5.538     6.303   496.5E6  110.6E6   59.398    61.614  
13) MA  Dieldrin        5.664     6.447   515.7E6  107.6E6   61.480    62.570  
14) MA  Endrin          5.921     6.661   482.7E6 94060929   60.201    62.445  
15) B   Endosulfa...    6.193     6.862   461.4E6 93808413   60.377    62.734  
16) A   4,4'-DDD        6.050     6.784   414.2E6 84356218   60.992    62.975  
17) MA  4,4'-DDT        6.287     7.083   438.7E6 82459833   60.322    63.528  
18) B   Endrin al...    6.362     6.985   378.2E6 78931751   59.481    61.873  
19) B   Endosulfa...    6.573     7.209   441.7E6 89617680   60.785    62.881  
20) A   Methoxychlor    6.835     7.539   237.2E6 47686113   59.374    60.985  
21) B   Endrin ke...    7.060     7.671   501.3E6 97122664   62.662    64.370  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.