Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033346.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 20:23 Operator : UA\AJ Sample : PEM Misc : ALS Vial : 3 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 23 23:11:52 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 13:36:10 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.985 113.9E6 32768135 19.323 20.270 28) SA Decachlor... 8.103 9.010 155.1E6 32989174 19.932 21.386 Target Compounds 2) A alpha-BHC 3.839 4.364 85138244 21320341 9.230 9.844 3) MA gamma-BHC... 4.120 4.644 82372467 21075868 9.896 10.450 6) B beta-BHC 4.371 4.806 37373969 10531291 9.963 10.577 12) B 4,4'-DDE 5.534 6.300 1143967 255601 0.137m 0.142m 14) MA Endrin 5.921 6.661 389.6E6 76459674 48.595 50.760 16) A 4,4'-DDD 6.052 6.782 7656677 1788707 1.127 1.335m 17) MA 4,4'-DDT 6.287 7.084 790.2E6 146.7E6 108.646 113.027 18) B Endrin al... 6.361 6.984 2388771 541830 0.376m 0.425m 20) A Methoxychlor 6.836 7.539 944.3E6 195.3E6 236.371 249.722 21) B Endrin ke... 7.061 7.669 8853270 3293484 1.107 2.183m# --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.