Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033347.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  20:38
  Operator  : UA\AJ
  Sample    : PSTDCCC050
  Misc      :  
  ALS Vial  : 4   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 23 23:12:01 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985   297.3E6 83756526   50.454    51.811  
28) SA  Decachlor...    8.103     9.010   375.2E6 77951516   48.228    50.534  

   Target Compounds
 2) A   alpha-BHC       3.839     4.364   477.9E6  115.7E6   51.808    53.405  
 3) MA  gamma-BHC...    4.119     4.644   436.7E6  106.5E6   52.462    52.812  
 4) MA  Heptachlor      4.409     5.158   447.2E6 99529119   50.936    51.384  
 5) MB  Aldrin          4.650     5.461   440.2E6 97189864   53.166    52.376  
 6) B   beta-BHC        4.371     4.806   192.2E6 51648287   51.250    51.871  
 7) B   delta-BHC       4.569     5.019   459.4E6  107.6E6   53.206    55.378m 
 8) B   Heptachlo...    5.090     5.839   403.1E6 94857198   50.319    57.157m 
 9) A   Endosulfan I    5.424     6.194   382.6E6 83371696   50.643    51.792  
10) B   gamma-Chl...    5.313     6.074   428.2E6 92252051   50.837    52.381  
11) B   alpha-Chl...    5.371     6.148   415.5E6 91215853   50.281    51.453  
12) B   4,4'-DDE        5.538     6.303   425.3E6 92837054   50.883    51.728  
13) MA  Dieldrin        5.664     6.447   427.5E6 89199442   50.971    51.886  
14) MA  Endrin          5.920     6.660   397.0E6 79126425   49.511    52.530m 
15) B   Endosulfa...    6.193     6.863   382.9E6 77991034   50.112    52.156  
16) A   4,4'-DDD        6.050     6.784   345.8E6 70622847   50.921    52.723  
17) MA  4,4'-DDT        6.287     7.083   355.1E6 66598121   48.819    51.308  
18) B   Endrin al...    6.362     6.985   311.7E6 65376381   49.025    51.247  
19) B   Endosulfa...    6.573     7.209   358.3E6 74050216   49.310    51.958  
20) A   Methoxychlor    6.835     7.538   193.7E6 39433936   48.491    50.432  
21) B   Endrin ke...    7.061     7.671   411.9E6 80501891   51.482    53.354  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.