Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033349.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 23 Feb 2018 21:08 Operator : UA\AJ Sample : J1635-01 Misc : ALS Vial : 26 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 23 23:12:22 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 13:36:10 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.985 108.5E6 31809328 18.417 19.677 28) SA Decachlor... 8.103 9.010 131.1E6 29526219 16.850 19.141 Target Compounds 12) B 4,4'-DDE 5.537 6.301 10665635 2175160 1.276m 1.212m --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.