Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033350.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  21:23
  Operator  : UA\AJ
  Sample    : J1635-01MS
  Misc      :  
  ALS Vial  : 27   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 23 23:12:31 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985   118.1E6 34217078   20.049    21.166  
28) SA  Decachlor...    8.104     9.011   128.8E6 28730383   16.553    18.625  

   Target Compounds
 2) A   alpha-BHC       3.839     4.364   600.5E6  147.4E6   65.097    68.063  
 3) MA  gamma-BHC...    4.119     4.644   543.9E6  135.2E6   65.344    67.058  
 4) MA  Heptachlor      4.408     5.158   545.4E6  122.6E6   62.121    63.291  
 5) MB  Aldrin          4.651     5.461   516.5E6  117.3E6   62.376    63.222  
 6) B   beta-BHC        4.371     4.806   235.2E6 64495646   62.714    64.773  
 7) B   delta-BHC       4.570     5.019   562.6E6  134.9E6   65.168    69.414m 
 8) B   Heptachlo...    5.091     5.841   488.7E6  108.3E6   61.013    65.259  
 9) A   Endosulfan I    5.424     6.194   446.3E6 99896377   59.073    62.057  
10) B   gamma-Chl...    5.314     6.074   501.9E6  107.3E6   59.594    60.933  
11) B   alpha-Chl...    5.372     6.148   484.2E6  108.1E6   58.586    60.991  
12) B   4,4'-DDE        5.538     6.304   478.0E6  107.9E6   57.189    60.145  
13) MA  Dieldrin        5.665     6.447   502.6E6  107.0E6   59.923    62.241  
14) MA  Endrin          5.921     6.661   472.8E6 92268735   58.970    61.255  
15) B   Endosulfa...    6.195     6.864   442.3E6 89817951   57.880    60.065  
16) A   4,4'-DDD        6.051     6.784   393.5E6 82208006   57.944    61.371  
17) MA  4,4'-DDT        6.288     7.084   410.2E6 77855117   56.402    59.980  
18) B   Endrin al...    6.363     6.985   348.6E6 75584738   54.826    59.249m 
19) B   Endosulfa...    6.574     7.209   413.5E6 85927960   56.899    60.292  
20) A   Methoxychlor    6.836     7.540   219.1E6 45557817   54.831    58.263  
21) B   Endrin ke...    7.061     7.672   475.2E6 93723377   59.400    62.117  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.