Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033351.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  21:38
  Operator  : UA\AJ
  Sample    : J1635-01MSD
  Misc      :  
  ALS Vial  : 28   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 23 23:12:52 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985   116.1E6 33713729   19.704    20.855  
28) SA  Decachlor...    8.104     9.011   130.2E6 28344609   16.729    18.375  

   Target Compounds
 2) A   alpha-BHC       3.840     4.365   589.3E6  145.4E6   63.890    67.122  
 3) MA  gamma-BHC...    4.120     4.644   531.8E6  133.2E6   63.887    66.068  
 4) MA  Heptachlor      4.409     5.159   534.7E6  121.1E6   60.911    62.525  
 5) MB  Aldrin          4.650     5.462   506.4E6  115.7E6   61.159    62.325  
 6) B   beta-BHC        4.371     4.806   229.6E6 63607203   61.216    63.881  
 7) B   delta-BHC       4.569     5.019   550.5E6  131.3E6   63.766    67.591m 
 8) B   Heptachlo...    5.091     5.840   478.7E6  110.8E6   59.759    66.749m 
 9) A   Endosulfan I    5.425     6.194   439.5E6 98921845   58.168    61.452  
10) B   gamma-Chl...    5.313     6.074   492.8E6  106.0E6   58.506    60.177  
11) B   alpha-Chl...    5.372     6.148   477.2E6  106.9E6   57.749    60.297  
12) B   4,4'-DDE        5.539     6.304   470.5E6  106.7E6   56.297    59.446  
13) MA  Dieldrin        5.665     6.447   495.4E6  105.6E6   59.066    61.416  
14) MA  Endrin          5.921     6.660   465.4E6 94098906   58.045    62.470m 
15) B   Endosulfa...    6.194     6.862   437.4E6 91459166   57.242    61.163m 
16) A   4,4'-DDD        6.051     6.784   386.7E6 80727590   56.933    60.266  
17) MA  4,4'-DDT        6.287     7.084   405.3E6 77893370   55.726    60.010  
18) B   Endrin al...    6.363     6.985   345.1E6 75014806   54.278    58.802m 
19) B   Endosulfa...    6.574     7.210   407.6E6 85002023   56.083    59.642  
20) A   Methoxychlor    6.835     7.540   217.6E6 45178812   54.472    57.779  
21) B   Endrin ke...    7.062     7.672   470.9E6 92253118   58.860    61.142  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.