Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033353.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  22:08
  Operator  : UA\AJ
  Sample    : PB106750BS
  Misc      :  
  ALS Vial  : 30   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 23 23:13:18 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985  93771425 27543568   15.915    17.038  
28) SA  Decachlor...    8.104     9.011   136.3E6 29036559   17.521    18.824  

   Target Compounds
 2) A   alpha-BHC       3.840     4.364   504.3E6  123.3E6   54.667    56.906  
 3) MA  gamma-BHC...    4.120     4.645   460.9E6  114.0E6   55.367    56.515  
 4) MA  Heptachlor      4.409     5.159   481.2E6  108.2E6   54.816    55.866  
 5) MB  Aldrin          4.651     5.462   459.6E6  104.6E6   55.504    56.382  
 6) B   beta-BHC        4.371     4.806   203.1E6 54993274   54.154    55.230  
 7) B   delta-BHC       4.570     5.020   486.3E6  116.5E6   56.322    59.942m 
 8) B   Heptachlo...    5.092     5.841   445.0E6 98707582   55.559    59.477  
 9) A   Endosulfan I    5.425     6.194   411.9E6 90726670   54.521    56.361  
10) B   gamma-Chl...    5.314     6.075   458.0E6 98985665   54.374    56.204  
11) B   alpha-Chl...    5.372     6.148   444.0E6 98745676   53.729    55.700  
12) B   4,4'-DDE        5.539     6.304   448.5E6  100.7E6   53.655    56.093  
13) MA  Dieldrin        5.666     6.447   462.3E6 97149131   55.121    56.510  
14) MA  Endrin          5.921     6.662   434.7E6 83913134   54.223    55.708  
15) B   Endosulfa...    6.194     6.863   415.3E6 84581528   54.343    56.564  
16) A   4,4'-DDD        6.052     6.784   373.5E6 76704498   54.996    57.263  
17) MA  4,4'-DDT        6.288     7.084   390.8E6 74046919   53.735    57.046  
18) B   Endrin al...    6.363     6.986   345.2E6 72629219   54.287    56.932  
19) B   Endosulfa...    6.574     7.209   394.9E6 80657320   54.343    56.594  
20) A   Methoxychlor    6.836     7.539   211.7E6 43607162   52.991    55.769  
21) B   Endrin ke...    7.062     7.672   456.3E6 88048435   57.036    58.355  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.