Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033355.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  22:39
  Operator  : UA\AJ
  Sample    : PB106796BS
  Misc      :  
  ALS Vial  : 32   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 23 23:13:43 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985  99147142 29485137   16.828    18.239  
28) SA  Decachlor...    8.104     9.012   143.7E6 30942929   18.470    20.059  

   Target Compounds
 2) A   alpha-BHC       3.839     4.364   534.5E6  132.1E6   57.940    60.989  
 3) MA  gamma-BHC...    4.120     4.645   489.5E6  122.2E6   58.801    60.572  
 4) MA  Heptachlor      4.409     5.158   508.6E6  115.4E6   57.936    59.575  
 5) MB  Aldrin          4.651     5.461   487.2E6  112.0E6   58.834    60.377  
 6) B   beta-BHC        4.372     4.805   215.5E6 58613884   57.443    58.866  
 7) B   delta-BHC       4.570     5.019   516.9E6  124.9E6   59.872    64.311m 
 8) B   Heptachlo...    5.091     5.841   461.4E6  105.8E6   57.606    63.737  
 9) A   Endosulfan I    5.425     6.193   435.3E6 96824122   57.612    60.149  
10) B   gamma-Chl...    5.313     6.074   484.7E6  106.0E6   57.543    60.181  
11) B   alpha-Chl...    5.371     6.148   470.2E6  105.6E6   56.891    59.545  
12) B   4,4'-DDE        5.538     6.303   470.3E6  107.2E6   56.270    59.727  
13) MA  Dieldrin        5.665     6.447   488.7E6  104.1E6   58.265    60.529  
14) MA  Endrin          5.921     6.660   455.7E6 92013951   56.837    61.086m 
15) B   Endosulfa...    6.194     6.863   440.6E6 90439527   57.663    60.481  
16) A   4,4'-DDD        6.051     6.784   395.5E6 82254729   58.238    61.406  
17) MA  4,4'-DDT        6.288     7.084   412.7E6 79053201   56.746    60.903  
18) B   Endrin al...    6.363     6.986   366.0E6 77453771   57.572    60.714  
19) B   Endosulfa...    6.574     7.209   416.7E6 86070589   57.346    60.392  
20) A   Methoxychlor    6.836     7.539   223.2E6 46185373   55.879    59.066  
21) B   Endrin ke...    7.061     7.671   485.3E6 94438263   60.664    62.590  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.