Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033358.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  23:24
  Operator  : UA\AJ
  Sample    : J1398-06MS
  Misc      :  
  ALS Vial  : 35   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 24 00:19:26 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.403     3.985   116.9E6 33648385   19.844    20.815  
28) SA  Decachlor...    8.104     9.011   162.7E6 34893673   20.908    22.621  

   Target Compounds
 2) A   alpha-BHC       3.840     4.365   558.8E6  138.5E6   60.576    63.957  
 3) MA  gamma-BHC...    4.120     4.645   515.3E6  127.6E6   61.911    63.292  
 4) MA  Heptachlor      4.409     5.159   516.5E6  116.3E6   58.839    60.056  
 5) MB  Aldrin          4.652     5.462   404.1E6  113.1E6   48.798    60.962  
 6) B   beta-BHC        4.372     4.807   224.4E6 60157899   59.825    60.417  
 7) B   delta-BHC       4.570     5.020   552.9E6  131.3E6   64.036    67.576m 
 8) B   Heptachlo...    5.092     5.840   486.0E6  110.5E6   60.673    66.578m 
 9) A   Endosulfan I    5.425     6.195   448.7E6 98736157   59.394    61.336  
10) B   gamma-Chl...    5.314     6.075   503.8E6  107.3E6   59.809    60.943  
11) B   alpha-Chl...    5.373     6.149   486.2E6  107.1E6   58.836    60.412  
12) B   4,4'-DDE        5.539     6.304   486.7E6  109.3E6   58.225    60.903  
13) MA  Dieldrin        5.666     6.448   510.4E6  106.3E6   60.851    61.837  
14) MA  Endrin          5.922     6.661   478.6E6 94628540   59.697    62.822m 
15) B   Endosulfa...    6.195     6.864   456.5E6 92443389   59.740    61.821  
16) A   4,4'-DDD        6.052     6.785   408.3E6 83501753   60.119    62.337  
17) MA  4,4'-DDT        6.288     7.084   430.5E6 81653267   59.186    62.906  
18) B   Endrin al...    6.364     6.987   376.6E6 78895756   59.236    61.845  
19) B   Endosulfa...    6.574     7.210   435.0E6 88410021   59.853    62.034  
20) A   Methoxychlor    6.836     7.540   234.0E6 47347191   58.560    60.552  
21) B   Endrin ke...    7.062     7.672   503.7E6 97406110   62.960    64.557  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.