Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033359.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 23 Feb 2018  23:39
  Operator  : UA\AJ
  Sample    : J1398-06MSD
  Misc      :  
  ALS Vial  : 36   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 24 00:19:41 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985   118.8E6 34189640   20.168    21.149  
28) SA  Decachlor...    8.104     9.011   164.4E6 34819470   21.128    22.572  

   Target Compounds
 2) A   alpha-BHC       3.840     4.363   567.5E6  140.4E6   61.521    64.806m 
 3) MA  gamma-BHC...    4.120     4.645   524.4E6  129.5E6   62.997    64.216  
 4) MA  Heptachlor      4.409     5.159   525.2E6  117.8E6   59.820    60.816  
 5) MB  Aldrin          4.651     5.462   409.6E6  114.4E6   49.468    61.654  
 6) B   beta-BHC        4.371     4.806   228.7E6 60913393   60.980    61.176  
 7) B   delta-BHC       4.570     5.020   561.7E6  136.1E6   65.061    70.030m 
 8) B   Heptachlo...    5.091     5.840   494.2E6  112.1E6   61.703    67.538m 
 9) A   Endosulfan I    5.425     6.194   456.9E6 99898914   60.469    62.059  
10) B   gamma-Chl...    5.314     6.074   511.4E6  109.0E6   60.716    61.885  
11) B   alpha-Chl...    5.372     6.148   494.5E6  108.1E6   59.834    60.998  
12) B   4,4'-DDE        5.538     6.304   497.2E6  110.7E6   59.482    61.660  
13) MA  Dieldrin        5.666     6.448   519.2E6  107.3E6   61.906    62.417  
14) MA  Endrin          5.921     6.660   489.6E6 95907792   61.066    63.671m 
15) B   Endosulfa...    6.194     6.864   464.7E6 92818452   60.815    62.072  
16) A   4,4'-DDD        6.051     6.784   415.4E6 84187516   61.158    62.849  
17) MA  4,4'-DDT        6.288     7.084   437.9E6 82708198   60.211    63.719  
18) B   Endrin al...    6.363     6.986   381.4E6 79890656   59.989    62.625  
19) B   Endosulfa...    6.574     7.210   441.9E6 89243153   60.807    62.618  
20) A   Methoxychlor    6.836     7.540   237.0E6 47893822   59.323    61.251  
21) B   Endrin ke...    7.062     7.672   510.6E6 98340717   63.827    65.177  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.