Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033368.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 24 Feb 2018  01:54
  Operator  : UA\AJ
  Sample    : PEM
  Misc      :  
  ALS Vial  : 3   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 24 02:48:30 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.403     3.985   109.5E6 32481272   18.586    20.093  
28) SA  Decachlor...    8.103     9.011   155.5E6 33403149   19.991m   21.654  

   Target Compounds
 2) A   alpha-BHC       3.840     4.364  82608061 21371193    8.956     9.867  
 3) MA  gamma-BHC...    4.120     4.644  78932302 21129093    9.483    10.477  
 6) B   beta-BHC        4.371     4.806  35863261 10619992    9.561    10.666  
12) B   4,4'-DDE        5.535     6.302   1701333    59176    0.204m    0.033m#
14) MA  Endrin          5.921     6.662   374.5E6 75985665   46.712    50.445  
16) A   4,4'-DDD        6.052     6.783   9168828  3266227    1.350     2.438m#
17) MA  4,4'-DDT        6.288     7.085   761.1E6  148.0E6  104.648   113.988  
18) B   Endrin al...    6.361     6.984   3368956   708476    0.530m    0.555m 
20) A   Methoxychlor    6.836     7.539   921.9E6  195.4E6  230.750   249.848  
21) B   Endrin ke...    7.060     7.670  11794561  3263120    1.474m    2.163m#
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.