Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033369.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 24 Feb 2018  02:09
  Operator  : UA\AJ
  Sample    : PSTDCCC050
  Misc      :  
  ALS Vial  : 4   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 24 02:48:39 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.403     3.986   283.9E6 83359950   48.178    51.566  
28) SA  Decachlor...    8.104     9.011   370.7E6 79357666   47.648    51.445  

   Target Compounds
 2) A   alpha-BHC       3.840     4.365   454.9E6  116.1E6   49.312    53.597  
 3) MA  gamma-BHC...    4.120     4.645   415.3E6  107.1E6   49.898    53.099  
 4) MA  Heptachlor      4.409     5.159   423.1E6  100.3E6   48.198    51.784  
 5) MB  Aldrin          4.651     5.462   410.2E6 98287001   49.535    52.967  
 6) B   beta-BHC        4.372     4.806   182.1E6 51654879   48.542    51.877  
 7) B   delta-BHC       4.570     5.020   429.4E6  108.9E6   49.740    56.070m 
 8) B   Heptachlo...    5.092     5.840   373.1E6 96056301   46.584    57.879m 
 9) A   Endosulfan I    5.425     6.194   349.5E6 84147143   46.259    52.273  
10) B   gamma-Chl...    5.314     6.074   406.2E6 92843069   48.225    52.717  
11) B   alpha-Chl...    5.372     6.148   386.0E6 92052269   46.702    51.924  
12) B   4,4'-DDE        5.537     6.304   378.2E6 93653865   45.250m   52.183  
13) MA  Dieldrin        5.666     6.447   393.6E6 90481671   46.925    52.632  
14) MA  Endrin          5.922     6.661   355.1E6 76753916   44.290    50.955  
15) B   Endosulfa...    6.194     6.863   359.9E6 78594106   47.094    52.559  
16) A   4,4'-DDD        6.052     6.784   324.5E6 71771461   47.782    53.580  
17) MA  4,4'-DDT        6.288     7.084   328.3E6 63069974   45.142    48.590  
18) B   Endrin al...    6.364     6.986   297.7E6 63437114   46.815    49.727  
19) B   Endosulfa...    6.574     7.210   342.8E6 74525340   47.172    52.291  
20) A   Methoxychlor    6.836     7.539   185.2E6 39348826   46.344    50.323  
21) B   Endrin ke...    7.062     7.672   408.2E6 82564206   51.026    54.721  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.