Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033371.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 24 Feb 2018 02:39 Operator : UA\AJ Sample : J1638-01 Misc : ALS Vial : 45 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 24 03:21:06 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 13:36:10 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.403 3.985 62091748 19077304 10.538 11.801 28) SA Decachlor... 8.104 9.012 98966525 21892619 12.720 14.192 Target Compounds 11) B alpha-Chl... 5.372 6.150 5763591 2840197 0.697 1.602m# 12) B 4,4'-DDE 5.537 6.302 27886900 7090738 3.337m 3.951m 17) MA 4,4'-DDT 6.287 7.082 12992048 2852524 1.786 2.198m --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.