Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033377.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 24 Feb 2018  04:09
  Operator  : UA\AJ
  Sample    : PB106785BS
  Misc      :  
  ALS Vial  : 51   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 24 04:39:22 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985   103.7E6 31318954   17.606    19.374  
28) SA  Decachlor...    8.105     9.011   157.8E6 32753789   20.283    21.233  

   Target Compounds
 2) A   alpha-BHC       3.840     4.364   551.9E6  140.8E6   59.834    64.989  
 3) MA  gamma-BHC...    4.120     4.645   505.2E6  129.4E6   60.697    64.182  
 4) MA  Heptachlor      4.409     5.159   517.6E6  120.4E6   58.956    62.173  
 5) MB  Aldrin          4.651     5.462   500.7E6  118.0E6   60.471    63.592  
 6) B   beta-BHC        4.371     4.806   221.2E6 61785751   58.976    62.052  
 7) B   delta-BHC       4.570     5.020   531.4E6  131.5E6   61.554    67.698m 
 8) B   Heptachlo...    5.092     5.841   468.1E6  110.7E6   58.444    66.725  
 9) A   Endosulfan I    5.425     6.195   445.6E6  101.3E6   58.982    62.909  
10) B   gamma-Chl...    5.314     6.075   496.1E6  111.1E6   58.896    63.071  
11) B   alpha-Chl...    5.372     6.149   481.2E6  110.3E6   58.230    62.239  
12) B   4,4'-DDE        5.539     6.304   481.3E6  112.4E6   57.581    62.618  
13) MA  Dieldrin        5.666     6.448   502.7E6  109.0E6   59.932    63.420  
14) MA  Endrin          5.922     6.662   465.6E6 92759188   58.077    61.581  
15) B   Endosulfa...    6.195     6.864   450.6E6 94951950   58.966    63.499  
16) A   4,4'-DDD        6.052     6.785   407.9E6 86779887   60.066    64.785  
17) MA  4,4'-DDT        6.288     7.085   416.2E6 81618813   57.225    62.880  
18) B   Endrin al...    6.364     6.986   373.0E6 81371299   58.672    63.785  
19) B   Endosulfa...    6.575     7.210   419.6E6 90354379   57.745    63.398  
20) A   Methoxychlor    6.837     7.540   224.6E6 47553021   56.206    60.815  
21) B   Endrin ke...    7.063     7.672   496.6E6 99599688   62.074    66.011  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.