Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033379.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 24 Feb 2018 04:39 Operator : UA\AJ Sample : PEM Misc : ALS Vial : 3 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 26 03:54:48 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 13:36:10 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.985 111.7E6 33419434 18.963 20.673 28) SA Decachlor... 8.104 9.012 160.2E6 33813506 20.590 21.920 Target Compounds 2) A alpha-BHC 3.839 4.364 83215898 21759807 9.021 10.047 3) MA gamma-BHC... 4.120 4.645 81122755 21509620 9.746 10.665 6) B beta-BHC 4.371 4.806 37132756 10726366 9.899 10.773 14) MA Endrin 5.922 6.662 378.9E6 76769127 47.254 50.965 16) A 4,4'-DDD 6.053 6.783 10247469 2145031 1.509 1.601m 17) MA 4,4'-DDT 6.289 7.083 780.8E6 150.2E6 107.357 115.707m 18) B Endrin al... 6.362 6.984 2845935 667948 0.448m 0.524m 20) A Methoxychlor 6.836 7.540 939.4E6 198.5E6 235.125 253.811 21) B Endrin ke... 7.060 7.671 10478403 2343436 1.310m 1.553m --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.