Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033380.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 24 Feb 2018  04:54
  Operator  : UA\AJ
  Sample    : PSTDCCC050
  Misc      :  
  ALS Vial  : 4   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 26 03:55:05 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.403     3.986   295.6E6 85982896   50.177    53.188  
28) SA  Decachlor...    8.104     9.012   387.9E6 80456281   49.855    52.157  

   Target Compounds
 2) A   alpha-BHC       3.840     4.365   476.1E6  119.3E6   51.615    55.088  
 3) MA  gamma-BHC...    4.120     4.645   437.2E6  109.9E6   52.523    54.483  
 4) MA  Heptachlor      4.409     5.159   447.5E6  102.5E6   50.973    52.933  
 5) MB  Aldrin          4.651     5.462   448.8E6  100.6E6   54.199    54.205  
 6) B   beta-BHC        4.371     4.806   193.1E6 53102514   51.475    53.331  
 7) B   delta-BHC       4.570     5.020   462.4E6  111.4E6   53.557    57.363m 
 8) B   Heptachlo...    5.091     5.841   410.0E6 98924718   51.185    59.608  
 9) A   Endosulfan I    5.425     6.194   384.1E6 86305234   50.839    53.614  
10) B   gamma-Chl...    5.314     6.075   431.6E6 95716708   51.241    54.348  
11) B   alpha-Chl...    5.372     6.148   416.2E6 94279681   50.362    53.181  
12) B   4,4'-DDE        5.538     6.304   434.6E6 94370741   51.993    52.583  
13) MA  Dieldrin        5.665     6.448   431.7E6 92367455   51.474    53.729  
14) MA  Endrin          5.921     6.662   396.5E6 78612684   49.447    52.189  
15) B   Endosulfa...    6.194     6.864   390.9E6 81022051   51.162    54.183  
16) A   4,4'-DDD        6.051     6.785   352.0E6 73562298   51.827    54.917  
17) MA  4,4'-DDT        6.288     7.085   354.8E6 68544304   48.786    52.807  
18) B   Endrin al...    6.364     6.987   317.2E6 68346286   49.885    53.575  
19) B   Endosulfa...    6.574     7.210   366.5E6 76528678   50.429    53.697  
20) A   Methoxychlor    6.836     7.540   193.2E6 39754344   48.359    50.841  
21) B   Endrin ke...    7.062     7.672   420.2E6 83726981   52.522    55.491  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.