Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033381.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 24 Feb 2018 05:09 Operator : UA\AJ Sample : J1396-01 10X Misc : ALS Vial : 52 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 26 03:55:30 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 13:36:10 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.403 3.984 5970362 1785528 1.013 1.105m 28) SA Decachlor... 8.105 9.010 6268003 1619662 0.806 1.050m# Target Compounds 12) B 4,4'-DDE 5.538 6.302 19761462 4989653 2.364 2.780m 17) MA 4,4'-DDT 6.288 7.083 13441151 3026104 1.848 2.331m# --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.