Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033390.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 24 Feb 2018 07:25 Operator : UA\AJ Sample : J1654-01 Misc : ALS Vial : 61 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 26 03:58:07 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 13:36:10 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.403 3.986 125.6E6 36133472 21.323 22.352 28) SA Decachlor... 8.104 9.012 112.1E6 25330086 14.414 16.421 Target Compounds 12) B 4,4'-DDE 5.539 6.305 1026.5E6 240.0E6 122.819 133.750 13) MA Dieldrin 5.666 6.447 67209713 15134248 8.013 8.803 16) A 4,4'-DDD 6.052 6.785 113.4E6 22980705 16.704 17.156 17) MA 4,4'-DDT 6.289 7.085 1153.2E6 232.6E6 158.551 179.228 --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.