Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033391.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 24 Feb 2018  07:40
  Operator  : UA\AJ
  Sample    : J1654-01MS
  Misc      :  
  ALS Vial  : 62   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 26 03:58:29 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985   132.6E6 38412405   22.513    23.762  
28) SA  Decachlor...    8.104     9.011   118.0E6 26868093   15.162    17.418  

   Target Compounds
 2) A   alpha-BHC       3.839     4.364   387.8E6  161.7E6   42.045    74.657 #
 3) MA  gamma-BHC...    4.120     4.643   567.5E6  149.4E6   68.182    74.097m 
 4) MA  Heptachlor      4.409     5.158   567.3E6  129.2E6   64.621    66.687  
 5) MB  Aldrin          4.651     5.461   518.7E6  122.0E6   62.645    65.727  
 6) B   beta-BHC        4.371     4.806   233.6E6 65952084   62.284    66.236  
 7) B   delta-BHC       4.569     5.022   549.7E6  472.0E6   63.668   242.915m#
 8) B   Heptachlo...    5.091     5.841   495.4E6  114.9E6   61.842    69.255  
 9) A   Endosulfan I    5.424     6.194   445.2E6  105.0E6   58.920    65.197  
10) B   gamma-Chl...    5.313     6.073   535.1E6  126.6E6   63.533    71.893  
11) B   alpha-Chl...    5.371     6.149   481.8E6  112.3E6   58.298    63.367  
12) B   4,4'-DDE        5.538     6.304  1474.1E6  343.3E6  176.364   191.295  
13) MA  Dieldrin        5.665     6.447   578.0E6  126.6E6   68.918    73.631  
14) MA  Endrin          5.921     6.661   555.0E6 86800398   69.217    57.625  
15) B   Endosulfa...    6.194     6.863   446.9E6 86728758   58.491    57.999  
16) A   4,4'-DDD        6.051     6.784   506.6E6  108.4E6   74.591    80.914  
17) MA  4,4'-DDT        6.287     7.084  1678.6E6  346.7E6  230.795   267.126  
18) B   Endrin al...    6.363     6.986   381.3E6 67724606   59.972    53.088  
19) B   Endosulfa...    6.574     7.209   390.8E6 88879579   53.772    62.363  
20) A   Methoxychlor    6.835     7.540   215.6E6 46346027   53.970    59.272  
21) B   Endrin ke...    7.061     7.672   468.4E6 97051651   58.547    64.323  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.