Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033392.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 24 Feb 2018  07:55
  Operator  : UA\AJ
  Sample    : J1654-01MSD
  Misc      :  
  ALS Vial  : 63   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 26 03:58:53 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.402     3.985   131.3E6 39188124   22.287    24.241  
28) SA  Decachlor...    8.104     9.011   124.0E6 27813693   15.938    18.031  

   Target Compounds
 2) A   alpha-BHC       3.838     4.364   662.5E6  165.1E6   71.819m   76.237  
 3) MA  gamma-BHC...    4.120     4.643   580.4E6  153.5E6   69.730    76.088m 
 4) MA  Heptachlor      4.409     5.159   577.7E6  131.8E6   65.808    68.040  
 5) MB  Aldrin          4.651     5.462   529.5E6  124.8E6   63.942    67.233  
 6) B   beta-BHC        4.371     4.806   239.2E6 67348798   63.763    67.639  
 7) B   delta-BHC       4.570     5.022   565.1E6  483.6E6   65.457   248.902m#
 8) B   Heptachlo...    5.091     5.841   507.7E6  119.2E6   63.388    71.827  
 9) A   Endosulfan I    5.425     6.194   453.4E6  107.1E6   60.011    66.538  
10) B   gamma-Chl...    5.313     6.074   549.6E6  128.7E6   65.252    73.085  
11) B   alpha-Chl...    5.372     6.149   491.9E6  114.9E6   59.523    64.828  
12) B   4,4'-DDE        5.539     6.304  1500.1E6  350.8E6  179.473   195.461  
13) MA  Dieldrin        5.665     6.448   589.4E6  129.6E6   70.275    75.382  
14) MA  Endrin          5.922     6.662   565.0E6 88154554   70.465    58.524  
15) B   Endosulfa...    6.194     6.864   457.5E6 87361789   59.875    58.423  
16) A   4,4'-DDD        6.052     6.785   519.3E6  111.5E6   76.461    83.234  
17) MA  4,4'-DDT        6.288     7.085  1698.5E6  354.0E6  233.522   272.736  
18) B   Endrin al...    6.364     6.987   391.0E6 69970424   61.501    54.848  
19) B   Endosulfa...    6.575     7.210   405.2E6 89707143   55.764    62.944  
20) A   Methoxychlor    6.836     7.540   219.3E6 47300060   54.902    60.492  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.