Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033393.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 24 Feb 2018 08:10 Operator : UA\AJ Sample : J1660-01 Misc : ALS Vial : 64 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 26 03:59:17 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 13:36:10 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.985 61173502 18020021 10.383 11.147 28) SA Decachlor... 8.104 9.011 63132263 12903338 8.114 8.365 Target Compounds 2) A alpha-BHC 3.837 4.362 5881756 1669139 0.638m 0.771m 3) MA gamma-BHC... 4.118 4.642 4774656 1496606 0.574m 0.742m# 4) MA Heptachlor 4.408 5.156 6230054 1327724 0.710 0.685m 5) MB Aldrin 4.651 5.459 5790784 1248164 0.699 0.673m 8) B Heptachlo... 5.090 5.839 5026880 1691836 0.628m 1.019m# 10) B gamma-Chl... 5.312 6.071 5095941 1473525 0.605m 0.837m# 11) B alpha-Chl... 5.371 6.148 8459581 2044966 1.024m 1.154m 12) B 4,4'-DDE 5.537 6.301 32801291 4195217 3.924m 2.338m# 13) MA Dieldrin 5.664 6.445 6484381 1431534 0.773m 0.833m 14) MA Endrin 5.921 6.659 8568249 1027397 1.069m 0.682m# 15) B Endosulfa... 6.195 6.862 9848180 1828874 1.289 1.223m 16) A 4,4'-DDD 6.051 6.781 6638395 1139328 0.977 0.851m 17) MA 4,4'-DDT 6.288 7.083 28770624 7868340 3.956 6.062m# 18) B Endrin al... 6.364 6.984 5070316 1087558 0.797m 0.853m 19) B Endosulfa... 6.574 7.207 7453523 1330818 1.026 0.934m 21) B Endrin ke... 7.061 7.668 5715025 1134275 0.714 0.752m --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.