Quantitation Report (QT Reviewed) Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\ Data File : PL033394.D Signal(s) : Signal #1: ECD1A.ch Signal #2: ECD2B.ch Acq On : 24 Feb 2018 08:25 Operator : UA\AJ Sample : J1660-06 Misc : ALS Vial : 65 Sample Multiplier: 1 Integration File signal 1: autoint1.e Integration File signal 2: autoint2.e Quant Time: Feb 26 03:59:39 2018 Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M Quant Title : GC Extractables QLast Update : Fri Feb 23 13:36:10 2018 Response via : Initial Calibration Integrator: ChemStation Volume Inj. : 2 µl Signal #1 Phase : ZB-MR1 Signal #2 Phase: ZB-MR2 Signal #1 Info : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm Compound RT#1 RT#2 Resp#1 Resp#2 ng/ml ng/ml --------------------------------------------------------------------------- System Monitoring Compounds 1) SA Tetrachlo... 3.402 3.985 113.3E6 33763948 19.236 20.886 28) SA Decachlor... 8.104 9.011 118.8E6 26867887 15.266 17.418 Target Compounds 17) MA 4,4'-DDT 6.287 7.082 8990078 1780153 1.236 1.371m --------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int.