Quantitation Report    (QT Reviewed)

  Data Path : P:\HPCHEM1\ECD_L\Data\PL022318\
  Data File : PL033397.D                                          
  Signal(s) : Signal #1: ECD1A.ch  Signal #2: ECD2B.ch
  Acq On    : 24 Feb 2018  09:10
  Operator  : UA\AJ
  Sample    : PSTDCCC050
  Misc      :  
  ALS Vial  : 4   Sample Multiplier: 1

  Integration File signal 1: autoint1.e
  Integration File signal 2: autoint2.e
  Quant Time: Feb 26 04:00:20 2018
  Quant Method : P:\HPCHEM1\ECD_L\methods\PL022318.M
  Quant Title  : GC Extractables
  QLast Update : Fri Feb 23 13:36:10 2018
  Response via : Initial Calibration
  Integrator: ChemStation

  Volume Inj.     : 2 µl
  Signal #1 Phase : ZB-MR1            Signal #2 Phase: ZB-MR2
  Signal #1 Info  : 30M x 0.32mm x0.5 Signal #2 Info : 30M x 0.32mm x0.25µm

        Compound         RT#1      RT#2    Resp#1   Resp#2   ng/ml    ng/ml
   ---------------------------------------------------------------------------

   System Monitoring Compounds
 1) SA  Tetrachlo...    3.403     3.986   307.8E6 88610834   52.235    54.814  
28) SA  Decachlor...    8.104     9.012   370.2E6 79599511   47.586    51.602  

   Target Compounds
 2) A   alpha-BHC       3.840     4.365   493.8E6  122.9E6   53.534    56.726  
 3) MA  gamma-BHC...    4.120     4.646   452.4E6  113.1E6   54.345    56.068  
 4) MA  Heptachlor      4.409     5.160   460.2E6  105.0E6   52.419    54.232  
 5) MB  Aldrin          4.651     5.462   461.5E6  103.0E6   55.731    55.513  
 6) B   beta-BHC        4.372     4.807   199.5E6 54509042   53.179    54.744  
 7) B   delta-BHC       4.570     5.020   477.7E6  114.1E6   55.323    58.733m 
 8) B   Heptachlo...    5.091     5.842   421.1E6  101.2E6   52.571    61.007  
 9) A   Endosulfan I    5.425     6.195   393.1E6 87990565   52.025    54.661  
10) B   gamma-Chl...    5.314     6.075   441.8E6 97660599   52.450    55.452  
11) B   alpha-Chl...    5.372     6.149   426.1E6 96262559   51.565    54.299  
12) B   4,4'-DDE        5.539     6.304   445.5E6 95860660   53.297    53.413  
13) MA  Dieldrin        5.666     6.448   440.3E6 94095466   52.495    54.734  
14) MA  Endrin          5.922     6.662   401.0E6 79295013   50.008    52.642  
15) B   Endosulfa...    6.195     6.865   395.4E6 82108255   51.742    54.910  
16) A   4,4'-DDD        6.052     6.786   357.3E6 74940938   52.608    55.946  
17) MA  4,4'-DDT        6.288     7.085   355.0E6 68599350   48.812    52.850  
18) B   Endrin al...    6.364     6.987   318.9E6 69258352   50.155    54.290  
19) B   Endosulfa...    6.575     7.210   366.9E6 77229031   50.492    54.188  
20) A   Methoxychlor    6.837     7.540   192.2E6 39861143   48.116    50.978  
21) B   Endrin ke...    7.061     7.673   449.3E6 85152867   56.162m   56.436  
   ---------------------------------------------------------------------------

  (f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25%  (m)=manual int.